ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

Base Information

Chemical Name:ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate
CAS No.:86632-10-2
Molecular Formula:C₃₅H₂₉N₅O₈
Molecular Weight:647.644
Hs Code.:

Synonyms:ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

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Chemical Property of ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

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Technology Process of ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

There total 2 articles about ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57018-83-4
O²,O³-dibenzoyl-1-(6-benzoylamino-purin-9-yl)-β-D-1-deoxy-arabinofuranose

: 86632-10-2
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

Guidance literature:: Multi-step reaction with 2 steps

1: DMSO, N,N'-dicyclohexylcarbodiimide (DCC), dichloroacetic acid

2: pyridine / 3 h

With pyridine; dichloro-acetic acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide;
DOI:10.1021/jm00364a033

Reference yield:

: 57018-84-5
N⁶-benzoyl-9-(β-D-arabino-2,3-di-O-benzoyl-1,5-pentodialdofuranosyl)adenine

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 86632-10-2
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

Guidance literature:: With pyridine; for 3h; Yield given;
DOI:10.1021/jm00364a033

Reference yield: 85.0%

: 86632-10-2
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

: 86632-11-3
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; acetic acid; for 32h; under 3102.9 Torr;
DOI:10.1021/jm00364a033