1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide

Base Information

Chemical Name:1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide
CAS No.:86632-15-7
Molecular Formula:C₃₃H₂₈N₆O₇
Molecular Weight:620.621
Hs Code.:

Synonyms:1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide

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Chemical Property of 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide

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Technology Process of 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide

There total 4 articles about 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57018-84-5
N⁶-benzoyl-9-(β-D-arabino-2,3-di-O-benzoyl-1,5-pentodialdofuranosyl)adenine

: 86632-15-7
1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3 h

2: 85 percent / H₂ / 10percent Pd/C / ethanol; acetic acid / 32 h / 3102.9 Torr

3: 1.) ammonia, trimethylaluminum / 1.) methylene chloride, toluene, RT, 5 min, 2.) methylene chloride, toluene, 42 deg C, 5 h

With pyridine; ammonia; hydrogen; trimethylaluminum; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1021/jm00364a033

Reference yield:

: 86632-10-2
ethyl 1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hept-5-eno-1,4-furanuronate

: 86632-15-7
1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / H₂ / 10percent Pd/C / ethanol; acetic acid / 32 h / 3102.9 Torr

2: 1.) ammonia, trimethylaluminum / 1.) methylene chloride, toluene, RT, 5 min, 2.) methylene chloride, toluene, 42 deg C, 5 h

With ammonia; hydrogen; trimethylaluminum; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1021/jm00364a033

Reference yield:

: 57018-83-4
O²,O³-dibenzoyl-1-(6-benzoylamino-purin-9-yl)-β-D-1-deoxy-arabinofuranose

: 86632-15-7
1-(6-benzamidopurin-9-yl)-1,5,6-trideoxy-2,3-di-O-benzoyl-β-D-arabino-hepto-1,4-furanuronamide

Guidance literature:: Multi-step reaction with 4 steps

1: DMSO, N,N'-dicyclohexylcarbodiimide (DCC), dichloroacetic acid

2: pyridine / 3 h

3: 85 percent / H₂ / 10percent Pd/C / ethanol; acetic acid / 32 h / 3102.9 Torr

4: 1.) ammonia, trimethylaluminum / 1.) methylene chloride, toluene, RT, 5 min, 2.) methylene chloride, toluene, 42 deg C, 5 h

With pyridine; dichloro-acetic acid; ammonia; hydrogen; trimethylaluminum; dimethyl sulfoxide; dicyclohexyl-carbodiimide; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1021/jm00364a033