2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol

Base Information

Chemical Name:2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol
CAS No.:1439365-40-8
Molecular Formula:C₂₇H₃₂N₆O₆
Molecular Weight:536.588
Hs Code.:

Synonyms:2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol

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Chemical Property of 2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol

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Technology Process of 2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol

There total 3 articles about 2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 49853-00-1
2,5-diethoxy-4-((4-nitrophenyl)diazenyl)aniline

: 91-99-6
N,N-dihydroxyethyl-m-toluidine

: 1439365-40-8
2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol

Guidance literature:: 2,5-diethoxy-4-((4-nitrophenyl)diazenyl)aniline; With nitrosylsulfuric acid; In 1-methyl-pyrrolidin-2-one; at 5 - 20 ℃; for 2h;

N,N-dihydroxyethyl-m-toluidine; In 1-methyl-pyrrolidin-2-one; water; butan-1-ol; at 20 ℃; Cooling with ice;

Reference yield:

: 94-85-9
2,5-diethoxyaniline

: 1439365-40-8
2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C / pH < 1

2.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 2 h / 5 - 20 °C

2.2: 20 °C / Cooling with ice

With hydrogenchloride; nitrosylsulfuric acid; sodium nitrite; In 1-methyl-pyrrolidin-2-one; water;

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 1439365-40-8
2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C / pH < 1

2.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 2 h / 5 - 20 °C

2.2: 20 °C / Cooling with ice

With hydrogenchloride; nitrosylsulfuric acid; sodium nitrite; In 1-methyl-pyrrolidin-2-one; water;