2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

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Chemical Name:2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)
CAS No.:1439365-41-9
Molecular Formula:C₃₃H₃₈Cl₂N₆O₈
Molecular Weight:717.606
Hs Code.:

Synonyms:2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

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Chemical Property of 2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

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Technology Process of 2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

There total 4 articles about 2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1439365-40-8
2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)diethanol

: 625-36-5
2-chloropropionyl chloride

: 1439365-41-9
2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 1439365-41-9
2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite; hydrogenchloride / water / 0 - 5 °C / pH < 1

2.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 2 h / 5 - 20 °C

2.2: 20 °C / Cooling with ice

3.1: potassium carbonate / tetrahydrofuran / 24 h / 20 °C

With hydrogenchloride; nitrosylsulfuric acid; potassium carbonate; sodium nitrite; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; water;

Reference yield:

: 49853-00-1
2,5-diethoxy-4-((4-nitrophenyl)diazenyl)aniline

: 1439365-41-9
2,2'-(4-((2,5-diethoxy-4-((4-nitrophenyl)diazenyl)phenyl)-diazenyl)-3-methylphenylazanediyl)bis(ethane-2,1-diyl) bis(3-chloropropanoate)

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitrosylsulfuric acid / 1-methyl-pyrrolidin-2-one / 2 h / 5 - 20 °C

1.2: 20 °C / Cooling with ice

2.1: potassium carbonate / tetrahydrofuran / 24 h / 20 °C

With nitrosylsulfuric acid; potassium carbonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;