4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile

Base Information

Chemical Name:4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile
CAS No.:141864-89-3
Molecular Formula:C₃₃H₂₉N₅
Molecular Weight:495.627
Hs Code.:

Synonyms:4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile

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Chemical Property of 4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile

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Technology Process of 4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile

There total 7 articles about 4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422043-21-7
C₁₉H₂₀N₄

: 114772-54-2
4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

: 141864-89-3
4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile

Guidance literature:: C₁₉H₂₀N₄; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 5h;
DOI:10.1002/cmdc.201200337

Reference yield:

: 37466-90-3
ethyl 3,4-diaminobenzoate

: 141864-89-3
4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 1 h / 20 °C

2.1: toluene-4-sulfonic acid / toluene / 3 h / Reflux

3.1: sodium hydroxide / methanol; water / 2 h / Reflux

4.1: polyphosphoric acid / 24 h / 150 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0 °C

5.2: 5 h / 0 - 20 °C

With sodium hydride; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/cmdc.201200337

Reference yield:

: 1433222-10-6
ethyl 3,4-dipentanamidobenzoate

: 141864-89-3
4-[(1'-methyl-2-butyl-2',6-bi-1H-benzo[d]imidazole-1-yl)methyl]biphenyl-2'-carbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 3 h / Reflux

2.1: sodium hydroxide / methanol; water / 2 h / Reflux

3.1: polyphosphoric acid / 24 h / 150 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0 °C

4.2: 5 h / 0 - 20 °C

With sodium hydride; toluene-4-sulfonic acid; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/cmdc.201200337