ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate

Base Information

Chemical Name:ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate
CAS No.:1246354-27-7
Molecular Formula:C₂₃H₂₄N₆O₇S₂
Molecular Weight:560.612
Hs Code.:

Synonyms:ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate

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Chemical Property of ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate

Chemical Property:

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Technology Process of ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate

There total 3 articles about ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 329904-04-3
3,5-diformyl-4-hydroxybenzoic acid ethyl ester

: 17852-52-7,27918-19-0
4-hydrazinobenzene-1-sulfonamide hydrochloride

: 1246354-27-7
ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate

Guidance literature:: With acetic acid; In ethanol; at 80 ℃; for 2h;
DOI:10.1021/jm300146f

Reference yield:

: 61660-77-3
ethyl 4-hydroxy-3,5-dimethylbenzoate

: 1246354-27-7
ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 18 h / 140 °C

2.1: chromium(VI) oxide; sulfuric acid; acetic anhydride; acetic acid / 22 h / 0 °C

2.2: 1 h / Reflux

3.1: acetic acid / ethanol / 2 h / 80 °C

With chromium(VI) oxide; sulfuric acid; acetic anhydride; acetic acid; In ethanol;
DOI:10.1021/jm300146f

Reference yield:

: 4919-37-3
3,5-dimethyl-4-hydroxybenzoic acid

: 1246354-27-7
ethyl 4-hydroxy-3,5-bis((2-(4-(aminosulfonyl)phenyl)hydrazinylidene)methyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 15 h / Reflux

2.1: 18 h / 140 °C

3.1: chromium(VI) oxide; sulfuric acid; acetic anhydride; acetic acid / 22 h / 0 °C

3.2: 1 h / Reflux

4.1: acetic acid / ethanol / 2 h / 80 °C

With chromium(VI) oxide; sulfuric acid; acetic anhydride; acetic acid; In ethanol;
DOI:10.1021/jm300146f