6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde

Base Information

Chemical Name:6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde
CAS No.:165537-93-9
Molecular Formula:C₁₈H₁₈ClNO₃S
Molecular Weight:363.865
Hs Code.:

Synonyms:6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde

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Chemical Property of 6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde

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Technology Process of 6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde

There total 2 articles about 6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32248-43-4
samarium diiodide

: Methyl 3-[6-(4-chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphth-1-yl]-2-propenoate

: 134937-92-1
4-benzyl-pyridine; dichromate

: 165537-93-9
6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; methanol; dichloromethane; chloroform; cyclohexane; ethyl acetate; methyl (triphenylphosphoranylidene)acetate;

Reference yield:

: 165537-90-6
6-(4-Chlorophenylsulfonyl)amino-2-oxo-5,6,7,8-tetrahydro-2H-benzo[e]pyran

: 23326-27-4
Methyl 2-butynoate

: 4-Chloro-N-(6-formyl-5-methyl-1,2,3,4-tetrahydro-naphthalen-2-yl)-benzenesulfonamide

: 165537-93-9
6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; 4-benzyl-pyridine; dichromate; Multistep reaction. Yields of byproduct given;
DOI:10.1016/S0960-894X(98)00220-0

Reference yield:

: 165537-93-9
6-(4-Chlorophenylsulfonyl)amino-2-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxaldehyde

: 165537-95-1
methyl 3-(6-(4-chlorophenylsulfonamido)-2-methyl-5,6,7,8-tetrahydronaphthalen-1-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / Heating

2: NaBH₄, CoCl₂ / methanol / 20 °C

With sodium tetrahydroborate; In methanol; toluene;
DOI:10.1016/S0960-894X(98)00220-0