N-(pyridin-2-yl)monomethyl terephthalate monoamide

Base Information

• Chemical Name: N-(pyridin-2-yl)monomethyl terephthalate monoamide
• CAS No.: 923748-45-2
• Molecular Formula: C₁₄H₁₂N₂O₃
• Molecular Weight: 256.261
• Mol file: 923748-45-2.mol

Synonyms:N-(pyridin-2-yl)monomethyl terephthalate monoamide

Chemical Property of N-(pyridin-2-yl)monomethyl terephthalate monoamide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N-(pyridin-2-yl)monomethyl terephthalate monoamide

There total 14 articles about N-(pyridin-2-yl)monomethyl terephthalate monoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-aminopyridine (504-29-0) + 4-Methoxycarbonylbenzoyl chloride (7377-26-6) → N-(pyridin-2-yl)monomethyl terephthalate monoamide (923748-45-2)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; for 24h;

DOI:10.1039/c2ce25995h

Reference yield: 89.0%

pyridin-3-ylamine (462-08-8) + 4-Methoxycarbonylbenzoyl chloride (7377-26-6) → N-(pyridin-2-yl)monomethyl terephthalate monoamide (923748-45-2)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1039/c2ce25995h

Reference yield: 82.0%

2-aminopyridine (504-29-0) + 4-ethynylbenzoic acid methyl ester (3034-86-4) → N-(pyridin-2-yl)monomethyl terephthalate monoamide (923748-45-2)

Guidance literature:

With oxygen; copper(l) chloride; In acetonitrile; at 20 ℃; for 18h; under 760.051 Torr; Irradiation;

DOI:10.1039/c6cc05506k

upstream raw materials:

2-aminopyridine

4-Methoxycarbonylbenzoyl chloride

pyridin-3-ylamine

1,4-benzenedicarboxylic acid dimethyl ester

Downstream raw materials:

4-chloro-N-(pyridine-2-yl)benzamide

N-(pyridin-2-yl)isonicotinamide

N-(1,2-diphenylethyl)pyridin-2-amine

2-(pivaloylamino)pyridine