Technology Process of C42H40BrN7O2
There total 4 articles about C42H40BrN7O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(II) acetate monohydrate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; dichloromethane; water;
at 20 ℃;
for 12h;
DOI:10.1021/jo3016659
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trichlorophosphate / acetonitrile / 1 h / Reflux
2: sodium L-ascorbate; copper(II) acetate monohydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / methanol; dichloromethane; water / 12 h / 20 °C
With
copper(II) acetate monohydrate; sodium L-ascorbate; trichlorophosphate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jo3016659
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide / methanol / 1 h
2: trichlorophosphate / acetonitrile / 1 h / Reflux
3: sodium L-ascorbate; copper(II) acetate monohydrate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / methanol; dichloromethane; water / 12 h / 20 °C
With
copper(II) acetate monohydrate; sodium L-ascorbate; potassium hydroxide; trichlorophosphate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jo3016659