33DIAMINO44DIMETHYLAZOXYBENZENE

Base Information

• Chemical Name: 33DIAMINO44DIMETHYLAZOXYBENZENE
• CAS No.: 5857-92-1
• Molecular Formula: C14H16N4O
• Molecular Weight: 256.307
• Mol file: 5857-92-1.mol

Synonyms:3,3'-Diamino-4,4'-dimethylazoxybenzene;3.3'-Diamino-4.4'-dimethyl-azoxybenzol;3,3'-Azoxybis(6-methylbenzenamine);Bis-(3-amino-4-methyl-phenyl)-diazen-N-oxid;6,6'-dimethyl-3,3'-azoxy-di-aniline;Benzenamine,3,3'-azoxybis(6-methyl;

Chemical Property of 33DIAMINO44DIMETHYLAZOXYBENZENE

Chemical Property:

• Vapor Pressure: 1.15E-10mmHg at 25°C
• Boiling Point: 513.8°C at 760 mmHg
• Flash Point: 264.5°C
• PSA: 93.15000
• Density: 1.24g/cm³
• LogP: 5.07910

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 33DIAMINO44DIMETHYLAZOXYBENZENE

There total 6 articles about 33DIAMINO44DIMETHYLAZOXYBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-5-nitroaniline (99-55-8) → 6,6'-dimethyl-3,3'-azoxy-di-aniline (5857-92-1)

Guidance literature:

With sodium amalgam; ethanol; acetic acid;

Reference yield:

2,4-dinitrotoluene (121-14-2) → 6,6'-dimethyl-3,3'-azoxy-di-aniline (5857-92-1)

Guidance literature:

Multi-step reaction with 2 steps

1: alcohol; ammonium sulfide

2: acetic acid; sodium amalgam; alcohol

With sodium amalgam; ammonium sulfide; ethanol; acetic acid;

Reference yield:

toluene (108-88-3,15644-74-3,16713-13-6) → 6,6'-dimethyl-3,3'-azoxy-di-aniline (5857-92-1)

Guidance literature:

Multi-step reaction with 3 steps

1: fuming nitric acid

2: alcohol; ammonium sulfide

3: acetic acid; sodium amalgam; alcohol

With sodium amalgam; ammonium sulfide; ethanol; nitric acid; acetic acid;

upstream raw materials:

2-methyl-5-nitroaniline

2,4-dinitrotoluene

toluene

o-toluidine

Downstream raw materials:

bis-(3-amino-4-methyl-phenyl)-diazene

bis-(3-acetylamino-4-methyl-phenyl)-diazene-N-oxide

4.6-diamino-m-cresol

4-methylbenzene-1,3-diamine