33DIAMINO44DIMETHYLAZOBENZENE

Base Information

• Chemical Name: 33DIAMINO44DIMETHYLAZOBENZENE
• CAS No.: 119631-00-4
• Molecular Formula: C₁₄H₁₆N₄
• Molecular Weight: 240.308
• Mol file: 119631-00-4.mol

Synonyms:o-Toluidine,5,5'-azobis- (2CI)

Chemical Property of 33DIAMINO44DIMETHYLAZOBENZENE

Chemical Property:

• Vapor Pressure: 2.33E-09mmHg at 25°C
• Boiling Point: 479.6°Cat760mmHg
• Flash Point: 243.8°C
• Density: 1.18g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 33DIAMINO44DIMETHYLAZOBENZENE

There total 6 articles about 33DIAMINO44DIMETHYLAZOBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-5-nitroaniline (99-55-8) → bis-(3-amino-4-methyl-phenyl)-diazene (119631-00-4)

Guidance literature:

Electrolysis_.elektrolytische Reduktion;

Reference yield:

6,6'-dimethyl-3,3'-azoxy-di-aniline (5857-92-1) → bis-(3-amino-4-methyl-phenyl)-diazene (119631-00-4)

Guidance literature:

With sodium amalgam; ethanol;

Reference yield:

2,4-dinitrotoluene (121-14-2) → bis-(3-amino-4-methyl-phenyl)-diazene (119631-00-4)

Guidance literature:

Multi-step reaction with 3 steps

1: alcohol; ammonium sulfide

2: acetic acid; sodium amalgam; alcohol

3: alcohol; sodium amalgam

With sodium amalgam; ammonium sulfide; ethanol; acetic acid;

upstream raw materials:

6,6'-dimethyl-3,3'-azoxy-di-aniline

2-methyl-5-nitroaniline

ethanol

2,4-dinitrotoluene

Downstream raw materials:

bis-(3-acetylamino-4-methyl-phenyl)-diazene