Technology Process of C27H25NO6
There total 5 articles about C27H25NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 20 ℃;
DOI:10.1021/jm800380b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere
1.2: -78 - 20 °C
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 2.5 h / 0 - 20 °C
2.2: 0 - 20 °C
3.1: ammonium cerium (IV) nitrate / water; acetonitrile / 0.5 h / 0 °C / Inert atmosphere
4.1: triethylamine; dmap / dichloromethane / 20 °C
With
dmap; ammonium cerium (IV) nitrate; methanesulfonyl chloride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
1.1: |Aldol Addition / 1.2: |Aldol Addition;
DOI:10.1021/acs.jmedchem.8b00661
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere
1.2: -78 - 20 °C
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 2.5 h / 0 - 20 °C
2.2: 0 - 20 °C
3.1: ammonium cerium (IV) nitrate / water; acetonitrile / 0.5 h / 0 °C / Inert atmosphere
4.1: triethylamine; dmap / dichloromethane / 20 °C
With
dmap; ammonium cerium (IV) nitrate; methanesulfonyl chloride; triethylamine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
1.1: |Aldol Addition / 1.2: |Aldol Addition;
DOI:10.1021/acs.jmedchem.8b00661
