1,3,5,7-tetrakis-(4-formylphenyl)adamantane

Base Information

• Chemical Name: 1,3,5,7-tetrakis-(4-formylphenyl)adamantane
• CAS No.: 645401-15-6
• Molecular Formula: C₃₈H₃₂O₄
• Molecular Weight: 552.67
• Mol file: 645401-15-6.mol

Synonyms:1,3,5,7-tetrakis-(4-formylphenyl)adamantane

Chemical Property of 1,3,5,7-tetrakis-(4-formylphenyl)adamantane

Chemical Property:

• Boiling Point: 735.0±60.0 °C(Predicted)
• Density: 1.309±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

1,3,5,7-tetrakis(4-formylphenyl)adamantane 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5,7-tetrakis-(4-formylphenyl)adamantane

There total 1 articles about 1,3,5,7-tetrakis-(4-formylphenyl)adamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Dichloromethyl methyl ether (4885-02-3) + 1,3,5,7-tetrakis(phenyl)adamantane (16004-75-4) → 1,3,5,7-tetrakis-(4-formylphenyl)adamantane (645401-15-6)

Guidance literature:

Dichloromethyl methyl ether; 1,3,5,7-tetrakis(phenyl)adamantane; With titanium tetrachloride; In dichloromethane; at -10 - 20 ℃; for 24h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; for 0.5h; Cooling with ice;

DOI:10.1016/j.tet.2011.10.052

Reference yield: 96.0%

1,3,5,7-tetrakis-(4-formylphenyl)adamantane (645401-15-6) → 1,3,5,7-tetrakis-(p-phenylmethanol)adamantane

Guidance literature:

With sodium tetrahydroborate; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1039/c7ta05004f

Reference yield: 90.0%

3,3',4,4'-tetraaminobiphenyl (91-95-2) + 1,3,5,7-tetrakis-(4-formylphenyl)adamantane (645401-15-6) → C86H72N16 (947369-36-0)

Guidance literature:

3,3',4,4'-tetraaminobiphenyl; 1,3,5,7-tetrakis-(4-formylphenyl)adamantane; In N,N-dimethyl acetamide; at 0 ℃;

With oxygen; In N,N-dimethyl acetamide; at 90 ℃; for 9h;

upstream raw materials:

Dichloromethyl methyl ether

1,3,5,7-tetrakis(phenyl)adamantane

Downstream raw materials:

C₈₆H₇₂N₁₆