pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate

Base Information

Chemical Name:pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate
CAS No.:928656-95-5
Molecular Formula:C₂₅H₁₅F₅N₂O₄S
Molecular Weight:534.463
Hs Code.:

Synonyms:pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate

Chemical Property:

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Technology Process of pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate

There total 7 articles about pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 928656-45-5
4-amino-5-bromo-3-biphenylcarboxamide

: 928656-94-4
pentafluorophenyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenesulfonate

: 928656-95-5
pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate

Guidance literature:: With borax; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; ethanol; for 16h; Heating / reflux;

Reference yield:

: 32658-67-6
2-amino-5-iodoanthranilamide

: 928656-95-5
pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. Na₂CO₃ / PdCl₂(dppf) / dioxane / 80 °C

2: NBS; acetic acid / 20 °C

3: aq. Na₂CO₃ / dioxane / 80 °C

With N-Bromosuccinimide; sodium carbonate; acetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; 1: Suzuki-Miyaura coupling / 3: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2007.04.088

Reference yield:

: 116027-10-2
5-iodoisatoic anhydride

: 928656-95-5
pentafluorophenyl 6'-amino-5'-(aminocarbonyl)-1,1':3',1''-terphenyl-4-sulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: ammonia / dioxane; tetrahydrofuran / 20 °C

2: aq. Na₂CO₃ / PdCl₂(dppf) / dioxane / 80 °C

3: NBS; acetic acid / 20 °C

4: aq. Na₂CO₃ / dioxane / 80 °C

With N-Bromosuccinimide; ammonia; sodium carbonate; acetic acid; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; 2: Suzuki-Miyaura coupling / 4: Suzuki-Miyaura coupling;
DOI:10.1016/j.bmcl.2007.04.088