N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine

Base Information

Chemical Name:N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine
CAS No.:104499-31-2
Molecular Formula:C₂₄H₃₄N₂O₅Si
Molecular Weight:458.63
Hs Code.:

Synonyms:N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine

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Chemical Property of N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine

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Technology Process of N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine

There total 4 articles about N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 104499-29-8
(4R,5S)-3-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-4-methyl-5-phenyl-1,3-oxazolidine-2-thione

: 104499-31-2
N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine

Guidance literature:: With triethylamine; In dichloromethane; for 72h; Ambient temperature;

Reference yield:

: 2768-56-1
Z-DL-serine

: 104499-31-2
N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) imidazole, 2) aq K₂CO₃ (10percent) / 1) DMF, 16 h, room temp., 2) MeOH, THF, 1 h, room temp.

2: 36.4 percent / WSC, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

3: 66 percent / Et₃N / CH₂Cl₂ / 72 h / Ambient temperature

With 1H-imidazole; dmap; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dichloromethane;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 104499-31-2
N-(N-benzyloxycarbonyl-O-dimethyl-t-butylsilyl-L-serinyl)-O-benzylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) imidazole, 2) aq K₂CO₃ (10percent) / 1) DMF, 16 h, room temp., 2) MeOH, THF, 1 h, room temp.

2: 36.4 percent / WSC, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

3: 66 percent / Et₃N / CH₂Cl₂ / 72 h / Ambient temperature

With 1H-imidazole; dmap; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dichloromethane;