1?phenyl?3?isopropylimidazolium bromide

Base Information

• Chemical Name: 1?phenyl?3?isopropylimidazolium bromide
• CAS No.: 700817-05-6
• Molecular Formula: Br*C₁₂H₁₅N₂
• Molecular Weight: 267.168
• Mol file: 700817-05-6.mol

Synonyms:1?phenyl?3?isopropylimidazolium bromide

Chemical Property of 1?phenyl?3?isopropylimidazolium bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1?phenyl?3?isopropylimidazolium bromide

There total 2 articles about 1?phenyl?3?isopropylimidazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

1-phenylimidazole (7164-98-9) + isopropyl bromide (75-26-3) → 1?phenyl?3?isopropylimidazolium bromide (700817-05-6)

Guidance literature:

In ethyl acetate; for 288h; Reflux;

DOI:10.1007/s10847-021-01082-6

Reference yield:

bromobenzene (108-86-1,52753-63-6) → 1?phenyl?3?isopropylimidazolium bromide (700817-05-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

1.2: 100 °C

2.1: ethyl acetate / 288 h / Reflux

With sodium hydroxide; In dimethyl sulfoxide; ethyl acetate;

DOI:10.1007/s10847-021-01082-6

Reference yield: 82.0%

dimethylsulfide gold(I) bromide (37922-40-0) + 1?phenyl?3?isopropylimidazolium bromide (700817-05-6) → bis(1?phenyl?3?isopropylimidazolin?2?ylidene) gold(I) bromide

Guidance literature:

1?phenyl?3?isopropylimidazolium bromide; With potassium carbonate; In acetonitrile; at 20 ℃; for 0.0833333h;

dimethylsulfide gold(I) bromide; In acetonitrile; for 24h;

DOI:10.1007/s10847-021-01082-6

upstream raw materials:

bromobenzene

1-phenylimidazole

isopropyl bromide