C₂₇H₃₁ClN₂O₂

Base Information

Chemical Name:C₂₇H₃₁ClN₂O₂
CAS No.:1421928-16-6
Molecular Formula:C₂₇H₃₁ClN₂O₂
Molecular Weight:451.008
Hs Code.:

C<sub>27</sub>H<sub>31</sub>ClN<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₇H₃₁ClN₂O₂

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Chemical Property of C₂₇H₃₁ClN₂O₂

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Technology Process of C₂₇H₃₁ClN₂O₂

There total 7 articles about C₂₇H₃₁ClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1421928-67-7
N-(1-(4-chloro-2-methylphenyl)-3-methylbutyl)-2-(4-hydroxyphenyl)acetamide

: 120277-68-1
2-methyl-3-(chloromethyl)pyridine

: 1421928-16-6
C₂₇H₃₁ClN₂O₂

Guidance literature:: With caesium carbonate; In acetonitrile; at 80 ℃; for 16h; Sealed tube;

Reference yield:

: 60032-57-7
2-methylnicotinaldehyde

: 1421928-16-6
C₂₇H₃₁ClN₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 10 h / 0 - 20 °C

2: thionyl chloride / dichloromethane / 2 h / 0 - 20 °C

3: caesium carbonate / acetonitrile / 16 h / 80 °C / Sealed tube

With thionyl chloride; sodium tris(acetoxy)borohydride; caesium carbonate; In dichloromethane; 1,2-dichloro-ethane; acetonitrile;

Reference yield:

: 50712-68-0
4-chloro-2-methylbenzonitrile

: 1421928-16-6
C₂₇H₃₁ClN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; diethyl ether / 5 h / 70 °C

2: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

3: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-methyl-morpholine / N,N-dimethyl-formamide / 4 h / 0 - 20 °C

4: caesium carbonate / acetonitrile / 16 h / 80 °C / Sealed tube

With 4-methyl-morpholine; sodium tetrahydroborate; caesium carbonate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide; acetonitrile;