N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride

Base Information

Chemical Name:N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride
CAS No.:1356146-31-0
Molecular Formula:C₄₇H₆₂N₅O₁₀*Cl
Molecular Weight:892.49
Hs Code.:

N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride

Synonyms:N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride

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Chemical Property of N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride

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Technology Process of N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride

There total 4 articles about N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 1356146-26-3
N-[9-(2-{[2-(tert-butylamino)-2-oxoethyl](2-{2-[2-(2-carboxy-ethoxy)ethoxy]ethoxy}ethyl)carbamoyl}phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

: 1356146-31-0
N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c1ob06581e

Reference yield:

: 252881-74-6,872340-65-3
tert-butyl 3-(2-(2-(2-aminoethoxyl)ethoxy)ethoxy)propanoate

: 1356146-31-0
N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 1 h / 100 °C / Microwave irradiation

2: phosphoric acid / toluene / 3 h / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

With dmap; phosphoric acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; toluene; 1: Ugi condensation;
DOI:10.1039/c1ob06581e

Reference yield:

: 1356146-21-8
N-[9-(2-([2-(tert-butylamino)-2-oxoethyl](14,14-dimethyl-12-oxo-3,6,9,13-tetraoxapentadec-1-yl)carbamoyl) phenyl)-6-(diethyl-amino)-3H-xanthen-3-ylidene]-N-ethylethanaminium chloride

: 1356146-31-0
N-(9-[2-([2-(tert-butylamino)-2-oxoethyl](2-[2-(2-( 3-[(2,5-dioxopyrrolidin-1-yl)oxy]-3-oxopropxy)ethoxy)ethoxy]ethyl)carbamoyl)phenyl]-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethyl-ethanaminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: phosphoric acid / toluene / 3 h / 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

With dmap; phosphoric acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; toluene;
DOI:10.1039/c1ob06581e