(E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate

Base Information

Chemical Name:(E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate
CAS No.:1291076-26-0
Molecular Formula:C₂₃H₃₀N₂O₇S
Molecular Weight:478.566
Hs Code.:

Synonyms:(E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate

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Chemical Property of (E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate

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Technology Process of (E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate

There total 5 articles about (E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1291076-25-9
C₇H₈ClNO₃

: 1291076-23-7
(E)-2-ethyl-2-hydroxy-N,N-diethyl-4-(phenylsulfonyl)but-3-enamide

: 1291076-26-0
(E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate

Guidance literature:: In tetrahydrofuran; hexane; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2011.02.017

Reference yield:

: C₁₉H₃₁NO₂SSi

: 1291076-26-0
(E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C / Inert atmosphere

3: tetrahydrofuran; hexane / 24 h / Inert atmosphere

With tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/j.tet.2011.02.017

Reference yield:

: 1291076-21-5
(E)-2-ethyl-2-hydroxy-N,N-diethyl-4-(phenylthio)but-3-enamide

: 1291076-26-0
(E)-3-(diethylcarbamoyl)-1-(phenylsulfonyl)pent-1-en-3-yl 3-oxo-3-(2-oxopyrrolidin-1-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: tetrahydrofuran; hexane / 24 h / Inert atmosphere

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1016/j.tet.2011.02.017