C₁₁H₁₂INO₂S

Base Information

Chemical Name:C₁₁H₁₂INO₂S
CAS No.:1420043-15-7
Molecular Formula:C₁₁H₁₂INO₂S
Molecular Weight:349.192
Hs Code.:

C<sub>11</sub>H<sub>12</sub>INO<sub>2</sub>S

Synonyms:C₁₁H₁₂INO₂S

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Chemical Property of C₁₁H₁₂INO₂S

Chemical Property:

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Technology Process of C₁₁H₁₂INO₂S

There total 3 articles about C₁₁H₁₂INO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 2-bromo-N-(2-iodophenyl)-N-methylacetamide

: 507-09-5
tiolacetic acid

: 1420043-15-7
C₁₁H₁₂INO₂S

Guidance literature:: tiolacetic acid; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h; Inert atmosphere;

2-bromo-N-(2-iodophenyl)-N-methylacetamide; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol303366u

Reference yield:

: 615-43-0
2-iodophenylamine

: 1420043-15-7
C₁₁H₁₂INO₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; dmap / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h / Inert atmosphere

3.1: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium hydride; caesium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol303366u

Reference yield:

: 1339628-12-4
N-(2-iodophenyl)-2-bromoacetamide

: 1420043-15-7
C₁₁H₁₂INO₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 0.5 h / Inert atmosphere

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With sodium hydride; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol303366u