(2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt

Base Information

Chemical Name:(2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt
CAS No.:1311287-63-4
Molecular Formula:C₂HF₃O₂*C₁₆H₁₄N₂O₅
Molecular Weight:428.322
Hs Code.:

Synonyms:(2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt

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Chemical Property of (2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt

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Technology Process of (2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt

There total 3 articles about (2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₂N₂O₅

: 76-05-1
trifluoroacetic acid

: 1311287-63-4
(2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt

Guidance literature:: at 20 ℃; for 0.25h;

Reference yield:

: 5904-71-2
methyl 5-formylfuran-2-carboxylate

: 1311287-63-4
(2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 0 - 20 °C

2.1: lithium hydroxide / water; methanol / 1.67 h / 20 °C

2.2: 0.17 h

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 20 °C

4.1: 0.25 h / 20 °C

With sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; pyridine; methanol; water;

Reference yield:

: 1311290-70-6
5-[(1E)-2-(tert-butoxycarbonyl)-prop-1-en-1-yl]furan-2-carboxylic acid methyl ester

: 1311287-63-4
(2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hydroxide / water; methanol / 1.67 h / 20 °C

1.2: 0.17 h

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 20 °C

3.1: 0.25 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In pyridine; methanol; water;