3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt

Base Information

Chemical Name:3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt
CAS No.:1311287-69-0
Molecular Formula:C₂HF₃O₂*C₁₆H₁₆N₂O₅
Molecular Weight:430.337
Hs Code.:

Synonyms:3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt

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Chemical Property of 3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt

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Technology Process of 3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt

There total 6 articles about 3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.3%

: 1311287-63-4
(2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt

: 76-05-1
trifluoroacetic acid

: 1311287-69-0
3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt

Guidance literature:: (2E)-3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropenoic acid trifluoroacetic acid salt; With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; under 760.051 Torr;

trifluoroacetic acid; In acetonitrile;

Reference yield:

: 13529-17-4
5-Formyl-2-furancarboxylic acid

: 1311287-69-0
3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 6 steps

1.1: hexane; acetone / 0.17 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

2.2: 0 - 20 °C

3.1: lithium hydroxide / water; methanol / 1.67 h / 20 °C

3.2: 0.17 h

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 20 °C

5.1: 0.25 h / 20 °C

6.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

With hydrogen; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; pyridine; methanol; hexane; water; acetone;

Reference yield:

: 5904-71-2
methyl 5-formylfuran-2-carboxylate

: 1311287-69-0
3-[5-(4-amidinophenoxycarbonyl)furan-2-yl]-2-methylpropionic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 0 - 20 °C

2.1: lithium hydroxide / water; methanol / 1.67 h / 20 °C

2.2: 0.17 h

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / pyridine / 20 °C

4.1: 0.25 h / 20 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

With hydrogen; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; pyridine; methanol; water;