2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt

Base Information

Chemical Name:2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt
CAS No.:541522-79-6
Molecular Formula:C₁₃H₂₃N₃O*ClH
Molecular Weight:273.806
Hs Code.:

Synonyms:2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt

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Chemical Property of 2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt

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Technology Process of 2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt

There total 2 articles about 2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: [2-(1-cyano-3-methyl-butylcarbamoyl)-cyclohexyl]-carbamic acid benzyl ester

: 541522-79-6
2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt

Guidance literature:: [2-(1-cyano-3-methyl-butylcarbamoyl)-cyclohexyl]-carbamic acid benzyl ester; With hydrogen; palladium 10% on activated carbon; In ethyl acetate; for 24h;

hydrogenchloride; In diethyl ether;

Reference yield:

: 680569-68-0
2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide

: 541522-79-6
2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt

Guidance literature:: With hydrogenchloride; In diethyl ether; water; for 24h;

Reference yield: 80.0%

: 3622-35-3
benzothiazole-6-carboxylic acid

: 541522-79-6
2-amino-cyclohexanecarboxylic acid (1-cyano-3-methyl-butyl)-amide hydrochloride salt

: N-[(1S,2R)-2-({[(1S)-1-cyano-3-methylbutyl]amino}carbonyl)cyclohexyl]-1,3-benzothiazole-6-carboxamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 24h;