2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid

Base Information

Chemical Name:2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid
CAS No.:1446476-01-2
Molecular Formula:C₄₁H₄₁N₅O₁₄
Molecular Weight:827.802
Hs Code.:

Synonyms:2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid

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Chemical Property of 2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid

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Technology Process of 2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid

There total 5 articles about 2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1446476-09-0
diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetate

: 1446476-01-2
2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid

Guidance literature:: diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetate; With potassium hydroxide; In tetrahydrofuran; water; at 20 ℃;

With acetic acid; In tetrahydrofuran; water;
DOI:10.1021/ic400465g

Reference yield:

: 1248447-17-7
N,N′-(pyridine-2,6-diylbis(methylene))dianiline

: 1446476-01-2
2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: dipotassium hydrogenphosphate; potassium iodide / acetonitrile / Reflux

2.1: trimethylsilyl trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / 7 h / -10 °C

2.2: 1 h

3.1: potassium hydroxide / tetrahydrofuran; water / 20 °C

With 2,6-dimethylpyridine; dipotassium hydrogenphosphate; trimethylsilyl trifluoromethanesulfonate; potassium iodide; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1021/ic400465g

Reference yield:

: 62-53-3
aniline

: 1446476-01-2
2,2′-((pyridine-2,6-diylbis(methylene))bis((4-((4,5-dimethoxy-2-nitrophenyl)(hydroxy)methyl)phenyl)azanediyl))diacetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: dipotassium hydrogenphosphate; potassium iodide / acetonitrile / Reflux

2.1: dipotassium hydrogenphosphate; potassium iodide / acetonitrile / Reflux

3.1: trimethylsilyl trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / 7 h / -10 °C

3.2: 1 h

4.1: potassium hydroxide / tetrahydrofuran; water / 20 °C

With 2,6-dimethylpyridine; dipotassium hydrogenphosphate; trimethylsilyl trifluoromethanesulfonate; potassium iodide; potassium hydroxide; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1021/ic400465g