diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate

Base Information

Chemical Name:diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate
CAS No.:1446476-08-9
Molecular Formula:C₂₇H₃₁N₃O₄
Molecular Weight:461.561
Hs Code.:

Synonyms:diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate

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Chemical Property of diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate

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Technology Process of diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate

There total 2 articles about diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.4%

: 1248447-17-7
N,N′-(pyridine-2,6-diylbis(methylene))dianiline

: 105-36-2
ethyl bromoacetate

: 1446476-08-9
diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate

Guidance literature:: With dipotassium hydrogenphosphate; potassium iodide; In acetonitrile; Reflux;
DOI:10.1021/ic400465g

Reference yield:

: 7703-74-4
2,6-bis-(bromomethyl)pyridine

: 1446476-08-9
diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: dipotassium hydrogenphosphate; potassium iodide / acetonitrile / Reflux

2: dipotassium hydrogenphosphate; potassium iodide / acetonitrile / Reflux

With dipotassium hydrogenphosphate; potassium iodide; In acetonitrile;
DOI:10.1021/ic400465g

Reference yield: 80.0%

: 1446476-08-9
diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate

: 1446476-11-4
2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetic acid

Guidance literature:: diethyl 2,2′-((pyridine-2,6-diylbis(methylene))bis(phenylazanediyl))diacetate; With potassium hydroxide; In tetrahydrofuran; water; at 20 ℃;

With acetic acid; In tetrahydrofuran; water;
DOI:10.1021/ic400465g