3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole

Base Information

Chemical Name:3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole
CAS No.:91476-96-9
Molecular Formula:C₂₂H₁₈N₂O₃S
Molecular Weight:390.463
Hs Code.:

Synonyms:3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole

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Chemical Property of 3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole

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Technology Process of 3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole

There total 1 articles about 3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 31271-90-6
1-(p-toluenesulfonyl)-1H-indole

: 698-16-8
benzohydroximoyl chloride

: 91476-96-9
3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole

Guidance literature:: With triethylamine; In diethyl ether; for 48h; Ambient temperature;

Reference yield:

: 91476-96-9
3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole

: 15224-25-6
3-benzoylindole

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH, 50percent H₂SO₄ (1 : 1) / 0.25 h / Heating

2: AcOH, 50percent H₂SO₄ (1 : 1) / 4 h / Heating

With sulfuric acid; acetic acid;

Reference yield:

: 91476-96-9
3-Phenyl-8-(toluene-4-sulfonyl)-8,8a-dihydro-3aH-isoxazolo[5,4-b]indole

: 67060-92-8
(1H-indole-1,3-diyl)bis(phenylmethanone)

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH, 50percent H₂SO₄ (1 : 1) / 0.25 h / Heating

2: AcOH, 50percent H₂SO₄ (1 : 1) / 4 h / Heating

3: 85 percent / Et₄NBr, NaOH / CH₂Cl₂ / 0.5 h / 0 °C

With sodium hydroxide; sulfuric acid; tetraethylammonium bromide; acetic acid; In dichloromethane;