(R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate

Base Information

Chemical Name:(R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate
CAS No.:1426820-63-4
Molecular Formula:C₁₆H₁₅Cl₃F₅NO₄
Molecular Weight:486.65
Hs Code.:

Synonyms:(R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate

Chemical Property:

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Technology Process of (R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate

There total 1 articles about (R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 136207-26-6,34702-60-8
N-(tert-butoxycarbonyl)-2,3,4,5,6-pentafluoro-D-phenylalanine

: 115-20-8
1,1,1-trichloroethanol

: 1426820-63-4
(R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate

Guidance literature:: With pyridine; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 20h;
DOI:10.3762/bjoc.8.231

Reference yield:

: 1426820-63-4
(R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate

: C₁₁H₇Cl₃F₅NO₂

Guidance literature:: (R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate; With trifluoroacetic acid; at 20 ℃; for 2h;

With sodium hydrogencarbonate; In dichloromethane;
DOI:10.3762/bjoc.8.231

Reference yield:

: 1426820-63-4
(R)-2,2,2-trichloroethyl 2-(tert-butoxycarbonylamino)-3-(pentafluorophenyl)-propanoate

: 1426820-64-5
(R)-2,2,2-trichloroethyl 2-acrylamido-3-(pentafluorophenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 2 h / 20 °C

2: triethylamine / dichloromethane / 7 h / 0 °C / Darkness

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.3762/bjoc.8.231