tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate

Base Information

• Chemical Name: tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate
• CAS No.: 1360603-61-7
• Molecular Formula: C₅₂H₅₇BrN₂O₂S₂
• Molecular Weight: 886.073

Synonyms:tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate

Chemical Property of tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate

Chemical Property:

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Technology Process of tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate

There total 1 articles about tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

1,3-dibromo-propane (109-64-8) + tert-butyl 2-(tritylthio) ethyl (2-(2-(tritylthio)ethylamino)ethyl)carbamate (549514-84-3) → tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate (1360603-61-7)

Guidance literature:

With potassium carbonate; In acetonitrile; for 18h; Reflux;

DOI:10.1021/jm201513c

Reference yield: 70.3%

2-(6-methylamino-3-pyridinyl)-1-benzofuran-5-ol (1054629-36-5) + tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate (1360603-61-7) → tert-butyl 2-((3-(2-(6-(methylamino)pyridin-3-yl)benzofuran-5-yloxy)propyl)(2-(tritylthio)ethyl)amino)ethyl(2-(tritylthio)ethyl)-carbamate (1360603-60-6)

Guidance literature:

With caesium carbonate; In acetone; for 5h; Reflux;

DOI:10.1021/jm201513c

Reference yield: 62.0%

tert-butyl (2-((3-bromopropyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate (1360603-61-7) + 2-(4-(dimethylamino)phenyl)quinoxalin-6-ol → tert-butyl (2-((3-((2-(4-(dimethylamino)phenyl)quinoxalin-6-yl)oxy)propyl)(2-(tritylthio)ethyl)amino)ethyl)(2-(tritylthio)ethyl)carbamate

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 2h;

DOI:10.1039/c6ra28395k

upstream raw materials:

1,3-dibromo-propane

tert-butyl 2-(tritylthio) ethyl (2-(2-(tritylthio)ethylamino)ethyl)carbamate

Downstream raw materials:

tert-butyl 2-((3-(2-(6-(methylamino)pyridin-3-yl)benzofuran-5-yloxy)propyl)(2-(tritylthio)ethyl)amino)ethyl(2-(tritylthio)ethyl)-carbamate

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