2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone

Base Information

Chemical Name:2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone
CAS No.:101601-64-3
Molecular Formula:C₁₇H₁₃N₃O₅S
Molecular Weight:371.373
Hs Code.:

Synonyms:2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone

Chemical Property:

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Technology Process of 2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone

There total 4 articles about 2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 27052-11-5
2-(4-nitrophenylimino)thiazolidin-4-one

: 121-33-5,8014-42-4
vanillin

: 101601-64-3
2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone

Guidance literature:: With sodium acetate; acetic acid; for 10h; Reflux;
DOI:10.1007/s00044-011-9730-1

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 101601-64-3
2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1: 4 h / 20 °C / Cooling with ice

2: ethanol / 5 h / Reflux

3: acetic acid; sodium acetate / 10 h / Reflux

With sodium acetate; acetic acid; In ethanol; 3: |Knoevenagel Condensation;
DOI:10.1007/s00044-011-9730-1

Reference yield:

: 17329-87-2
2-chloro-N-(4-nitro-phenyl)-acetamide

: 101601-64-3
2-(4-nitrophenylimino)-5-(4-hydroxy-3-methoxybenzylidene)-4-thiazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / Reflux

2: acetic acid; sodium acetate / Reflux

With sodium acetate; acetic acid; In ethanol; 2: |Knoevenagel Condensation;
DOI:10.1007/s00044-018-02288-z