N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride

Base Information

Chemical Name:N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride
CAS No.:1202552-62-2
Molecular Formula:C₁₃H₁₂BrN₃*ClH
Molecular Weight:326.623
Hs Code.:

Synonyms:N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride

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Chemical Property of N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride

Chemical Property:

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Technology Process of N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride

There total 1 articles about N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 350-03-8
methyl-3-pyridylketone

: 622-88-8,41931-18-4
4-bromophenylhydrazine hydrochloride

: 1202552-62-2
N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride

Guidance literature:: In ethanol; at 90 ℃; for 3h;

Reference yield:

: 1202552-62-2
N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride

: 1202549-63-0
1-(3,5-dimethyl-benzoyl)-2-pyridin-3-yl-1H-indole-5-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: PPA / 1 h / 210 °C

2.1: 1-methyl-pyrrolidin-2-one / 160 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran / 0.67 h / 0 - 20 °C

3.2: 0 - 20 °C

With PPA; sodium hydride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;

Reference yield:

: 1202552-62-2
N-(4-bromo-phenyl)-N-[1-pyridin-3-yl-eth-(Z)-ylidene]-hydrazine hydrochloride

: 1202549-52-7
1-(3-cyano-benzoyl)-2-pyridin-3-yl-1H-indole-5-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: PPA / 1 h / 210 °C

2.1: 1-methyl-pyrrolidin-2-one / 160 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / 20 °C

3.2: Inert atmosphere

With PPA; potassium hexamethylsilazane; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; toluene;