allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate

Base Information

Chemical Name:allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate
CAS No.:1052213-60-1
Molecular Formula:C₄₂H₄₉NO₇Si
Molecular Weight:707.939
Hs Code.:

Synonyms:allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate

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Chemical Property of allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate

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Technology Process of allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate

There total 1 articles about allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1052213-57-6
allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-(hydroxymethyl)-4-oxohexanoate

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1052213-60-1
allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo801258h

Reference yield: 65.0%

: 1052213-60-1
allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate

: 1052213-63-4
allyl (5S)-5-((benzyloxycarbonyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate

Guidance literature:: allyl (5S)-5-((benzyloxycarbonyl)(4-methoxybenzyl)amino)-2-((tert-butyldiphenylsilyloxy)methyl)-4-oxohexanoate; With ammonium cerium (IV) nitrate; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

With water; In tetrahydrofuran; Inert atmosphere;
DOI:10.1021/jo801258h