2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester

Base Information

• Chemical Name: 2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester
• CAS No.: 844892-98-4
• Molecular Formula: C₂₉H₂₉NO₃
• Molecular Weight: 439.554

Synonyms:2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester

Chemical Property of 2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester

Chemical Property:

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Technology Process of 2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester

There total 1 articles about 2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

methyl 2-bromo-3-cyclohexyl-1H-indole-6-carboxylate (494799-19-8) + [4-(benzyloxy)phenyl]boronic acid (146631-00-7) → 2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester (844892-98-4)

Guidance literature:

With potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; In ethanol; water; toluene; at 80 ℃; for 12h;

Reference yield: 80.5%

2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester (844892-98-4) + bromoacetic acid methyl ester (96-32-2) → C32H33NO5 (1165793-78-1)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.33333h;

Reference yield:

2-(4-benzyloxyphenyl)-3-cyclohexyl-1H-indole-6-carboxylic acid methyl ester (844892-98-4) + methyl iodide (74-88-4) → C30H31NO3

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃;

DOI:10.1016/j.bmcl.2007.03.027

upstream raw materials:

methyl 2-bromo-3-cyclohexyl-1H-indole-6-carboxylate

[4-(benzyloxy)phenyl]boronic acid

Downstream raw materials:

C₂₃H₂₅NO₃

C₃₈H₄₃N₃O₅

C₃₂H₃₃NO₅

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