2-bromophenyl phenyl sulfide

Base Information

• Chemical Name: 2-bromophenyl phenyl sulfide
• CAS No.: 15861-48-0
• Molecular Formula: C₁₂H₉BrS
• Molecular Weight: 265.173
• Mol file: 15861-48-0.mol

Synonyms:2-bromophenyl phenyl sulfide

Chemical Property of 2-bromophenyl phenyl sulfide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-bromophenyl phenyl sulfide

There total 21 articles about 2-bromophenyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-Bromo-2-iodobenzene (583-55-1) + thiophenol (108-98-5) → 2-bromophenyl phenyl sulfide (15861-48-0)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; bis[2-(diphenylphosphino)phenyl] ether; In toluene; for 3h; Reflux; Inert atmosphere;

DOI:10.1021/jacs.8b06730

Reference yield: 97.0%

iodobenzene (591-50-4) + o-bromothiophenol (6320-02-1) → 2-bromophenyl phenyl sulfide (15861-48-0)

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; potassium tert-butylate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In toluene; at 50 ℃; for 72h;

DOI:10.1016/j.tet.2008.04.108

Reference yield: 93.0%

1-Bromo-2-iodobenzene (583-55-1) + diphenyldisulfane (882-33-7) → 2-bromophenyl phenyl sulfide (15861-48-0)

Guidance literature:

With copper(I) sulfide; iron; potassium carbonate; In dimethyl sulfoxide; at 120 ℃;

upstream raw materials:

2-carboxybenzene diazonium chloride

2-(2-Bromo-phenylsulfanylmethyl)-furan

thiophenol

2-bromoaniline

Downstream raw materials:

1-(2-Phenylsulfanyl-phenyl)-cyclopropanol

2-(phenylsulfonyl)benzonitrile

1-bromo-2-(phenylsulfonyl)benzene

1-phenyl-1-<2-(phenylthio)phenyl>ethene