N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide

Base Information

Chemical Name:N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide
CAS No.:1235871-31-4
Molecular Formula:C₃₂H₂₄BrNO₅
Molecular Weight:582.45
Hs Code.:

Synonyms:N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide

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Chemical Property of N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide

Chemical Property:

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Technology Process of N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide

There total 5 articles about N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1235871-30-3
1-amino-5-(biphenyl[1,1']-4-yl)-2,3-dimethoxynaphthalene

: 957765-79-6
6-bromo-2,3-(methylenedioxy)benzoyl chloride

: 1235871-31-4
N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2012.09.097

Reference yield:

: 1235871-28-9
1-bromo-5-nitro-2,3-dimethoxynaphthalene

: 1235871-31-4
N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene / 90 °C

2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 85 °C

3: triethylamine / dichloromethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; sodium carbonate; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; water; toluene; 1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.09.097

Reference yield:

: 5122-94-1
4-biphenylboronic acid

: 1235871-31-4
N-(5-([1,1'-biphenyl]-4-yl)-6,7-dimethoxynaphthalen-1-yl)-5-bromobenzo[d][1,3]dioxole-4-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; toluene / 90 °C

2: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 85 °C

3: triethylamine / dichloromethane / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; sodium carbonate; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; water; toluene; 1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.09.097