Technology Process of C24H26N6O5S
There total 11 articles about C24H26N6O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dimethyl sulfoxide;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: O,O-Diethyl hydrogen phosphorodithioate / ethanol; water / 100 °C / Inert atmosphere
2.1: dihydrogen peroxide / ethanol / 22 h / Inert atmosphere
3.1: potassium carbonate / tetrahydrofuran; dimethyl sulfoxide / 0.25 h / 20 °C
3.2: 20 °C
4.1: sulfuric acid / 1.83 h / 45 °C
4.2: Cooling with ice
5.1: sodium tetrahydroborate / tetrahydrofuran / Reflux
5.2: 2 h / Reflux
6.1: pyridine / 2.16 h / 20 °C
7.1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; N,N-dimethyl-formamide / 24 h / 4137.29 Torr / Autoclave
8.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran; dimethyl sulfoxide / 2 h / 20 °C
With
pyridine; sodium tetrahydroborate; sulfuric acid; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; potassium carbonate; O,O-Diethyl hydrogen phosphorodithioate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: dihydrogen peroxide / ethanol / 22 h / Inert atmosphere
2.1: potassium carbonate / tetrahydrofuran; dimethyl sulfoxide / 0.25 h / 20 °C
2.2: 20 °C
3.1: sulfuric acid / 1.83 h / 45 °C
3.2: Cooling with ice
4.1: sodium tetrahydroborate / tetrahydrofuran / Reflux
4.2: 2 h / Reflux
5.1: pyridine / 2.16 h / 20 °C
6.1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; N,N-dimethyl-formamide / 24 h / 4137.29 Torr / Autoclave
7.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran; dimethyl sulfoxide / 2 h / 20 °C
With
pyridine; sodium tetrahydroborate; sulfuric acid; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;