3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate

Base Information

Chemical Name:3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate
CAS No.:1446246-94-1
Molecular Formula:C₁₆H₁₉N₅O₄S
Molecular Weight:377.424
Hs Code.:

Synonyms:3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate

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Chemical Property of 3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate

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Technology Process of 3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate

There total 10 articles about 3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1446246-93-0
3-[({[4-(aminocarbonyl)-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate

: 1446246-94-1
3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate

Guidance literature:: 3-[4-({[(4-methylphenyl)amino]carbonyl}amino)phenyl]-5-{[(2-oxopyrrolidin-1-yl)carbonyl]amino}isothiazol-4-carboxamide; With sodium hydroxide; at 20 ℃;

With hydrogenchloride; In water;

Reference yield:

: 605661-26-5
2-[amino(4-nitrophenyl)methylene]malononitrile

: 1446246-94-1
3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: O,O-Diethyl hydrogen phosphorodithioate / ethanol; water / 100 °C / Inert atmosphere

2.1: dihydrogen peroxide / ethanol / 22 h / Inert atmosphere

3.1: potassium carbonate / tetrahydrofuran; dimethyl sulfoxide / 0.25 h / 20 °C

3.2: 20 °C

4.1: sulfuric acid / 1.83 h / 45 °C

4.2: Cooling with ice

5.1: sodium tetrahydroborate / tetrahydrofuran / Reflux

5.2: 2 h / Reflux

6.1: pyridine / 2.16 h / 20 °C

7.1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; N,N-dimethyl-formamide / 24 h / 4137.29 Torr / Autoclave

With pyridine; sodium tetrahydroborate; sulfuric acid; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; potassium carbonate; O,O-Diethyl hydrogen phosphorodithioate; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 909028-96-2
3-amino-3-(4-nitrophenyl)-2-thioformamidoacrylonitrile

: 1446246-94-1
3-[({[4-(aminocarbonyl)-3-(4-aminophenyl)isothiazol-5-yl]amino}carbonyl)amino]propyl acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: dihydrogen peroxide / ethanol / 22 h / Inert atmosphere

2.1: potassium carbonate / tetrahydrofuran; dimethyl sulfoxide / 0.25 h / 20 °C

2.2: 20 °C

3.1: sulfuric acid / 1.83 h / 45 °C

3.2: Cooling with ice

4.1: sodium tetrahydroborate / tetrahydrofuran / Reflux

4.2: 2 h / Reflux

5.1: pyridine / 2.16 h / 20 °C

6.1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; N,N-dimethyl-formamide / 24 h / 4137.29 Torr / Autoclave

With pyridine; sodium tetrahydroborate; sulfuric acid; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;