C₂₂H₃₅N₃O₆Si

Base Information

Chemical Name:C₂₂H₃₅N₃O₆Si
CAS No.:1268625-02-0
Molecular Formula:C₂₂H₃₅N₃O₆Si
Molecular Weight:465.622
Hs Code.:

C<sub>22</sub>H<sub>35</sub>N<sub>3</sub>O<sub>6</sub>Si

Synonyms:C₂₂H₃₅N₃O₆Si

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Chemical Property of C₂₂H₃₅N₃O₆Si

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Technology Process of C₂₂H₃₅N₃O₆Si

There total 8 articles about C₂₂H₃₅N₃O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1268625-01-9
C₂₀H₃₃N₃O₅Si

: 108-24-7
acetic anhydride

: 1268625-02-0
C₂₂H₃₅N₃O₆Si

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 - 20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ol2000765

Reference yield:

: 679412-06-7
tert-butyl ((2R,6R)-6-methyl-5-oxo-5,6-dihydro-2H-pyran-2-yl) carbonate

: 1268625-02-0
C₂₂H₃₅N₃O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 1.83 h / -78 - 0 °C / Inert atmosphere

3: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 21.08 h / 0 - 20 °C / Inert atmosphere

4: 1H-imidazole / tetrahydrofuran; dichloromethane / 0.33 h / 0 °C / Inert atmosphere

5: sodium azide; lithium perchlorate / acetonitrile / 20.5 h / 80 °C / Inert atmosphere

6: pyridine; dmap / dichloromethane / 0.33 h / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; sodium azide; cerium(III) chloride heptahydrate; lithium perchlorate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol2000765

Reference yield:

: 247244-64-0
(2R)-6-hydroxy-2-methyl-2H-pyran-3-(6H)-one

: 1268625-02-0
C₂₂H₃₅N₃O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: dmap / dichloromethane / 14 h / -78 - -30 °C / Inert atmosphere

2: triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

3: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol; dichloromethane / 1.83 h / -78 - 0 °C / Inert atmosphere

4: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 21.08 h / 0 - 20 °C / Inert atmosphere

5: 1H-imidazole / tetrahydrofuran; dichloromethane / 0.33 h / 0 °C / Inert atmosphere

6: sodium azide; lithium perchlorate / acetonitrile / 20.5 h / 80 °C / Inert atmosphere

7: pyridine; dmap / dichloromethane / 0.33 h / 0 - 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; dmap; sodium tetrahydroborate; sodium azide; cerium(III) chloride heptahydrate; lithium perchlorate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ol2000765