1-Methyl-1-nitrocyclohexane

Base Information

• Chemical Name: 1-Methyl-1-nitrocyclohexane
• CAS No.: 59368-15-9
• Molecular Formula: C₇H₁₃NO₂
• Molecular Weight: 143.186
• Mol file: 59368-15-9.mol

Synonyms:1-Methyl-1-nitrocyclohexane

Chemical Property of 1-Methyl-1-nitrocyclohexane

Chemical Property:

• Melting Point: -71°C
• Refractive Index: 1.4598 (estimate)
• Boiling Point: 261.28°C (rough estimate)
• Density: 1.0384

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Methyl-1-nitrocyclohexane

There total 12 articles about 1-Methyl-1-nitrocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1-Methylcyclohexanol (590-67-0) → 1-Methyl-1-nitrocyclohexane (59368-15-9)

Guidance literature:

With hydrogenchloride; acetic acid; sodium nitrite; In dichloromethane; at 20 ℃; for 5h;

Reference yield:

methyl cyclohexane (82166-21-0) → Adipic acid (124-04-9) + 1-Methyl-1-nitrocyclohexane (59368-15-9) + 1-methyl-3-nitro-cyclohexane (127818-60-4)

Guidance literature:

Reference yield:

nitric acid (7697-37-2,78989-43-2) + methyl cyclohexane (82166-21-0) → Adipic acid (124-04-9) + 1-Methyl-1-nitrocyclohexane (59368-15-9) + 1-methyl-3-nitro-cyclohexane (127818-60-4)

Guidance literature:

upstream raw materials:

1-methyl-1-cyclohexylamine

methyl cyclohexane

nitric acid

diethyl ether

Downstream raw materials:

1,1'-Dimethyl-azoxycyclohexan

benzyl-(1-methyl-cyclohexyl)-amine

methyl-(1-methyl-cyclohexyl)-amine

dimethyl-(1-methyl-cyclohexyl)-amine