(S)-3-(dimethylamino)-2-methyl-1-(3-nitrophenyl)-propan-1-one (2R,3R)-O,O'-dibenzoyltartrate

Base Information

Chemical Name:(S)-3-(dimethylamino)-2-methyl-1-(3-nitrophenyl)-propan-1-one (2R,3R)-O,O'-dibenzoyltartrate
CAS No.:1309956-64-6
Molecular Formula:C₁₂H₁₆N₂O₃*C₁₈H₁₄O₈
Molecular Weight:594.575
Hs Code.:

Synonyms:(S)-3-(dimethylamino)-2-methyl-1-(3-nitrophenyl)-propan-1-one (2R,3R)-O,O'-dibenzoyltartrate

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Chemical Property of (S)-3-(dimethylamino)-2-methyl-1-(3-nitrophenyl)-propan-1-one (2R,3R)-O,O'-dibenzoyltartrate

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Technology Process of (S)-3-(dimethylamino)-2-methyl-1-(3-nitrophenyl)-propan-1-one (2R,3R)-O,O'-dibenzoyltartrate

There total 2 articles about (S)-3-(dimethylamino)-2-methyl-1-(3-nitrophenyl)-propan-1-one (2R,3R)-O,O'-dibenzoyltartrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.2%

: 53013-01-7
3-(dimethylamino)-2-methyl-1-(3-nitro-phenyl)-propan-1-one

: 2743-38-6
O,O'-dibenzoyl-L-tartaric acid

: 1309956-64-6
(S)-3-(dimethylamino)-2-methyl-1-(3-nitrophenyl)-propan-1-one (2R,3R)-O,O'-dibenzoyltartrate

Guidance literature:: In methanol; acetone; at 20 - 40 ℃;

Reference yield:

: 17408-16-1
3'-nitropropiophenone

: 1309956-64-6
(S)-3-(dimethylamino)-2-methyl-1-(3-nitrophenyl)-propan-1-one (2R,3R)-O,O'-dibenzoyltartrate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / water / 1.5 h / 50 - 70 °C

1.2: 16 h / 70 °C

1.3: pH 10 - 12

2.1: acetone; methanol / 20 - 40 °C

With acetic anhydride; In methanol; water; acetone; 1.1: Mannich Reaction / 1.2: Mannich Reaction;