NN-dimethyl-N-phenacylanilinium bromide

Base Information

Chemical Name:NN-dimethyl-N-phenacylanilinium bromide
CAS No.:16042-85-6
Molecular Formula:Br*C₁₆H₁₈NO
Molecular Weight:320.229
Hs Code.:

Synonyms:NN-dimethyl-N-phenacylanilinium bromide

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Chemical Property of NN-dimethyl-N-phenacylanilinium bromide

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Technology Process of NN-dimethyl-N-phenacylanilinium bromide

There total 1 articles about NN-dimethyl-N-phenacylanilinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 70-11-1
α-bromoacetophenone

: 16042-85-6
NN-dimethyl-N-phenacylanilinium bromide

Guidance literature:: DOI:10.1039/P19810001154

Reference yield: 80.0%

: 16042-85-6
NN-dimethyl-N-phenacylanilinium bromide

: anhydro

Guidance literature:: With sodium hydroxide; at 0 ℃;
DOI:10.1039/P19810001154

Reference yield:

: 3375-31-3
palladium diacetate

: 16042-85-6
NN-dimethyl-N-phenacylanilinium bromide

: thallium(I) 2,4-pentanedionate

: 1353014-47-7
[Pd(C₆H₄COCHN(CH₃)2C₆H₅)(CH₃COCHCOCH₃)]

: 1353014-49-9
[Pd₂(C₆H₄COCHN(CH₃)2C₆H₄)(CH₃COCHCOCH₃)2]

Guidance literature:: With LiCl; In methanol; dichloromethane; toluene; byproducts: TlCl; to a suspn. of a ligand (0.545 mmol) in toluene was added Pd-contg. compd. (0.545 mmol); stirring at 60°C for 2 h; the solid obtained wasreacted in MeOH with an excess of LiCl (2.02 mmol) for 2 h; treatment w ith Tl(acac) (1.09 mmol) in CH2Cl2; after stirring for 25 min at 25°C, the soln. was filtered and evapd. to dryness; the residue was treated with cold n-pentane; elem. anal.;
DOI:10.1021/om201001c