succinic acid monobenzhydryl ester

Base Information

• Chemical Name: succinic acid monobenzhydryl ester
• CAS No.: 128925-50-8
• Molecular Formula: C₁₇H₁₆O₄
• Molecular Weight: 284.312
• Mol file: 128925-50-8.mol

Synonyms:succinic acid monobenzhydryl ester

Chemical Property of succinic acid monobenzhydryl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of succinic acid monobenzhydryl ester

There total 4 articles about succinic acid monobenzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

succinic acid benzhydryl ester 1,2,3,4-tetrahydro-naphthalen-1-yl ester → succinic acid monobenzhydryl ester (128925-50-8)

Guidance literature:

With chloro-trimethyl-silane; sodium iodide; In acetonitrile; at 20 ℃; for 1.5h;

DOI:10.1016/S0040-4039(99)01040-0

Reference yield: 31.0%

succinic acid (110-15-6) + diazodiphenylmethane (908093-98-1) → succinic acid monobenzhydryl ester (128925-50-8)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1039/b923814j

Reference yield: 26.0%

succinic acid anhydride (108-30-5) + 1,1-Diphenylmethanol (91-01-0) → succinic acid monobenzhydryl ester (128925-50-8)

Guidance literature:

at 180 - 190 ℃; for 6h;

DOI:10.1021/jo00305a013

upstream raw materials:

succinic acid anhydride

1,1-Diphenylmethanol

succinic acid

diazodiphenylmethane

Downstream raw materials:

<1-(Ethoxycarbonyl)-4-<(diphenylmethoxy)carbonyl>-2-oxobutylidene>triphenylphosphorane

3-((diphenylmethoxy)carbonyl)propionyl chloride

Refernces

• 1、 Slade, Christopher J.,Pringle, Carol A.,Sumner, Ian G.. "1,2,3,4-Tetrahydro-1-naphthyl ester as a selective protecting group for carboxylic acids". . p. 5601 - 5604. Retrieved 2007/10/03.