C₃₂H₃₀N₄O₄S

Base Information

Chemical Name:C₃₂H₃₀N₄O₄S
CAS No.:1261277-10-4
Molecular Formula:C₃₂H₃₀N₄O₄S
Molecular Weight:566.681
Hs Code.:

C<sub>32</sub>H<sub>30</sub>N<sub>4</sub>O<sub>4</sub>S

Synonyms:C₃₂H₃₀N₄O₄S

Suppliers and Price of C₃₂H₃₀N₄O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₃₀N₄O₄S

Chemical Property:

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Technology Process of C₃₂H₃₀N₄O₄S

There total 12 articles about C₃₂H₃₀N₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 123-75-1
pyrrolidine

: 1261277-08-0
C₂₈H₂₂BrN₃O₄S

: 1261277-10-4
C₃₂H₃₀N₄O₄S

Guidance literature:: at 20 ℃; for 16h;

Reference yield:

: 24310-36-9
1-tosyl-2,3,4,5-tetrahydro-1H-1-benzazepin-5-one

: 1261277-10-4
C₃₂H₃₀N₄O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: trichlorophosphate / 5 h / 20 °C / Reflux

1.2: Cooling with ice

2.1: ethanol; sodium / 0.5 h / Cooling with ice

2.2: 3.5 h / 0 °C / Reflux

3.1: hydrogen bromide; acetic acid / Reflux

3.2: 6 h / Reflux

4.1: thionyl chloride / 70 °C

4.2: 3 h / 760.05 Torr

5.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 50 °C

6.1: zinc; acetic acid / acetonitrile / 6 h

7.1: potassium carbonate; isobutyl chloroformate / tetrahydrofuran / 1 h

7.2: 72 h

8.1: 16 h / 20 °C

With dmap; thionyl chloride; ethanol; hydrogen bromide; sodium; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; trichlorophosphate; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 50998-74-8
methyl N-tosylanthranilate

: 1261277-10-4
C₃₂H₃₀N₄O₄S

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / butanone, 1-

2.1: potassium tert-butylate / toluene

3.1: trichlorophosphate / 5 h / 20 °C / Reflux

3.2: Cooling with ice

4.1: ethanol; sodium / 0.5 h / Cooling with ice

4.2: 3.5 h / 0 °C / Reflux

5.1: hydrogen bromide; acetic acid / Reflux

5.2: 6 h / Reflux

6.1: thionyl chloride / 70 °C

6.2: 3 h / 760.05 Torr

7.1: dmap; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 50 °C

8.1: zinc; acetic acid / acetonitrile / 6 h

9.1: potassium carbonate; isobutyl chloroformate / tetrahydrofuran / 1 h

9.2: 72 h

10.1: 16 h / 20 °C

With dmap; thionyl chloride; ethanol; potassium tert-butylate; hydrogen bromide; sodium; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; trichlorophosphate; isobutyl chloroformate; In tetrahydrofuran; butanone, 1-; N,N-dimethyl-formamide; toluene; acetonitrile;