N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide

Base Information

Chemical Name:N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide
CAS No.:1621584-37-9
Molecular Formula:C₁₆H₁₁Cl₂N₃O₃
Molecular Weight:364.188
Hs Code.:

Synonyms:N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide

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Chemical Property of N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide

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Technology Process of N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide

There total 4 articles about N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 150544-04-0
6-amino-1,3-dihydro-indol-2-one

: 10278-20-3
3,4-dichlorobenzoyl isocyanate

: 1621584-37-9
N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide

Guidance literature:: In acetonitrile; at 70 - 80 ℃;
DOI:10.1016/j.ejmech.2014.07.108

Reference yield:

: 643-43-6
(2,4-dinitro-phenyl)-acetic acid

: 1621584-37-9
N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; palladium on activated charcoal / methanol

2: hydrogenchloride / water / 6 h / Reflux

3: acetonitrile / 70 - 80 °C

With hydrogenchloride; palladium on activated charcoal; hydrogen; In methanol; water; acetonitrile;
DOI:10.1016/j.ejmech.2014.07.108

Reference yield:

: 79637-84-6
2,4-diaminophenylacetic acid

: 1621584-37-9
N-(2-oxoindolin-6-ylcarbamoyl)-3,4-dichlorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 6 h / Reflux

2: acetonitrile / 70 - 80 °C

With hydrogenchloride; In water; acetonitrile;
DOI:10.1016/j.ejmech.2014.07.108