2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride

Base Information

Chemical Name:2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride
CAS No.:138688-21-8
Molecular Formula:C₆₁H₄₉ClO₁₇
Molecular Weight:1089.5
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride

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Chemical Property of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride

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Technology Process of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride

There total 1 articles about 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 138688-20-7
[(2R,3R,4S,5R,6R)-3,4,5-tribenzoyloxy-6-[[(2R,3R,4S,5R,6R)-3,4,5-tribenzoyloxy-6-[cyano(phenyl)methoxy]tetrahydropyran-2-yl]methoxy]tetrahydropyran-2-yl]methyl benzoate

: 138688-21-8
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride

Guidance literature:: With Dichloromethyl methyl ether; zinc(II) chloride; In chloroform; for 14h; Molecular sieve; Inert atmosphere; Reflux;
DOI:10.1039/c5cc04773k

Reference yield: 97.0%

: 31367-69-8
potassium p-tolylthiolate

: 138688-21-8
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride

: p-methylphenyl O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1→6)-2,3,4-tri-O-benzoyl-1-thio-β-D- glucopyranoside

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1039/c5cc04773k

Reference yield: 68.0%

: 143249-67-6
Methyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzoyl-β-D-glucopyranoside

: 138688-21-8
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1,6)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl chloride

: 143249-71-2
Methyl O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzoyl-β-D-glu..)

Guidance literature:: With 2,4,6-trimethyl-pyridine; 3 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90575-5