(S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate

Base Information

Chemical Name:(S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate
CAS No.:1439619-16-5
Molecular Formula:C₁₅H₂₆NO₇PS₂
Molecular Weight:427.48
Hs Code.:

(S<sub>S</sub>,R<sub>C</sub>)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate

Synonyms:(S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate

Chemical Property:

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Technology Process of (S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate

There total 5 articles about (S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1439619-04-1
(S_S,R_C)-diethyl [3-hydroxy-2-(p-tolylsulfinylamino)propane]phosphonate

: 124-63-0
methanesulfonyl chloride

: 1439619-16-5
(S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/ejoc.201201589

Reference yield:

: 683-08-9
Diethyl methylphosphonate

: 1439619-16-5
(S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

1.2: 5 h / -78 °C

2.1: ozone / methanol; dichloromethane / 0.25 h / -78 °C

3.1: sodium tetrahydroborate / 5 h / -78 - 20 °C

4.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

With sodium tetrahydroborate; ozone; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/ejoc.201201589

Reference yield:

: 181136-73-2
C₁₆H₁₅NOS

: 1439619-16-5
(S_S,R_C)-diethyl [3-mesyloxy-2-(p-tolylsulfinylamino)propane]phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

1.2: 5 h / -78 °C

2.1: ozone / methanol; dichloromethane / 0.25 h / -78 °C

3.1: sodium tetrahydroborate / 5 h / -78 - 20 °C

4.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

With sodium tetrahydroborate; ozone; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/ejoc.201201589