3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate

Base Information

Chemical Name:3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate
CAS No.:1415747-39-5
Molecular Formula:C₃₂H₃₄NO₆P
Molecular Weight:559.599
Hs Code.:

Synonyms:3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate

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Chemical Property of 3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate

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Technology Process of 3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate

There total 5 articles about 3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1415747-25-9
dibenzyl 3-(N-(benzyloxy)acetamido)-1-hydroxypropylphosphonate

: 108-95-2,27073-41-2
phenol

: 1415747-39-5
3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 30 ℃; Sonication;
DOI:10.1021/jm301577q

Reference yield:

: 1373213-82-1
tert-butyl N-(benzyloxy)-N-(but-3-enyl)carbamate

: 1415747-39-5
3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium iodide / methanol; acetonitrile / 1 h / 20 °C

1.2: 1.08 h / 0 - 20 °C

2.1: potassium osmate(VI) dihydrate; sodium periodate / tetrahydrofuran; water / 4 h / Darkness

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C

3.2: 0.25 h / -78 °C

4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 30 °C / Sonication

With potassium osmate(VI) dihydrate; sodium periodate; di-isopropyl azodicarboxylate; triphenylphosphine; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1021/jm301577q

Reference yield:

: 1415747-26-0
N-(benzyloxy)-N-(2-formylethyl)acetamide

: 1415747-39-5
3-(N-dibenzyl 3-(N-(benzyloxy)acetamido))-1-phenoxypropylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C

1.2: 0.25 h / -78 °C

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 30 °C / Sonication

With di-isopropyl azodicarboxylate; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/jm301577q