tert-butyl-2,6-diethylphenylcarbamate

Base Information

• Chemical Name: tert-butyl-2,6-diethylphenylcarbamate
• CAS No.: 129464-02-4
• Molecular Formula: C₁₅H₂₃NO₂
• Molecular Weight: 249.353

Synonyms:tert-butyl-2,6-diethylphenylcarbamate

Chemical Property of tert-butyl-2,6-diethylphenylcarbamate

Chemical Property:

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Technology Process of tert-butyl-2,6-diethylphenylcarbamate

There total 1 articles about tert-butyl-2,6-diethylphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.9%

2,6-diethylaniline (579-66-8) + di-tert-butyl dicarbonate (24424-99-5) → tert-butyl-2,6-diethylphenylcarbamate (129464-02-4)

Guidance literature:

In water; for 48h;

DOI:10.1002/anie.200802910

Reference yield: 77.3%

tert-butyl-2,6-diethylphenylcarbamate (129464-02-4) + 1,2,3-oxathiazolidine-3-carboxylic acid, 4-phenyl 1,1-dimethylethyl ester-2,2-dioxide (479687-23-5) → (S)-N1-(2,6-diethylphenyl)-2-phenylethane-1,2-diamine (1083004-75-4)

Guidance literature:

tert-butyl-2,6-diethylphenylcarbamate; 1,2,3-oxathiazolidine-3-carboxylic acid, 4-phenyl 1,1-dimethylethyl ester-2,2-dioxide; With sodium hydride; In N,N-dimethyl-formamide; for 12h;

With sulfuric acid; In 1,4-dioxane; at 22 ℃; for 48h;

DOI:10.1002/anie.200802910

Reference yield:

tert-butyl-2,6-diethylphenylcarbamate (129464-02-4) + 2-(benzyloxy)-4-fluoro-1-nitrobenzene (129464-01-3) → N-t-Butoxycarbonyl-6,4-(2,6-diethylphenyl)amino-2-benzyloxynitrobenzene

Guidance literature:

In N-methyl-acetamide; water;

upstream raw materials:

2,6-diethylaniline

di-tert-butyl dicarbonate

Downstream raw materials:

(S)-N₁-(2,6-diethylphenyl)-2-phenylethane-1,2-diamine

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