(4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

Base Information

• Chemical Name: (4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane
• CAS No.: 1402010-09-6
• Molecular Formula: C₂₃H₃₄BClO₂
• Molecular Weight: 388.786

Synonyms:(4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

Chemical Property of (4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

Chemical Property:

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Technology Process of (4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

There total 1 articles about (4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dichloromethane (75-09-2) + (4S,5S)-4,5-dicyclohexyl-2-phenethyl-1,3,2-dioxaborolane (1402010-08-5) → (4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane (1402010-09-6)

Guidance literature:

dichloromethane; (4S,5S)-4,5-dicyclohexyl-2-phenethyl-1,3,2-dioxaborolane; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -40 ℃; for 0.166667h;

With zinc(II) chloride; at -40 - 20 ℃; for 2h;

DOI:10.1021/acs.orglett.1c03164

Reference yield: 100.0%

(4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane (1402010-09-6) + cinnamylzinc bromide lithium chloride → (4S,5S)-4,5-dicyclohexyl-2-[(S,E)-1,6-diphenylhex-5-en-3-yl]-1,3,2-dioxaborolane

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 18h;

DOI:10.1021/acs.orglett.1c03164

Reference yield: 99.0%

(4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane (1402010-09-6) + allylmagnesium bromide (1730-25-2) → (4S,5S)-4,5-dicyclohexyl-2-[(S)-1-phenylhex-5-en-3-yl]-1,3,2-dioxaborolane

Guidance literature:

In diethyl ether; dichloromethane; at -78 ℃; for 1h;

DOI:10.1021/acs.orglett.1c03164

upstream raw materials:

dichloromethane

(4S,5S)-4,5-dicyclohexyl-2-phenethyl-1,3,2-dioxaborolane

Downstream raw materials:

C₂₃H₂₄O₂

C₂₃H₂₁F₃O

C₂₄H₂₄O₃

C₂₇H₃₁NO₃

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