2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride

Base Information

Chemical Name:2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride
CAS No.:140903-18-0
Molecular Formula:C₁₃H₁₈N₂O₂S*ClH
Molecular Weight:302.825
Hs Code.:

Synonyms:2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride

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Chemical Property of 2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride

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Technology Process of 2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride

There total 3 articles about 2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 33876-09-4
2-(benzyloxycarbonylamino)-propionitrile

: 75-08-1
ethanethiol

: 140903-18-0
2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; at 0 ℃;

Reference yield:

: 17343-54-3
(S)-2-(benzyloxycarbonylamino)-propionitrile

: 75-08-1
ethanethiol

: 140903-18-0
(S)-2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; at -8 ℃; for 0.5h;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 140903-18-0
2-Benzyloxycarbonylamino-thiopropionimidic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / NaOH / CH₂Cl₂; H₂O / 0.08 h / 0 °C

2: 95 percent / gaseous HCl / diethyl ether / 0 °C

With hydrogenchloride; sodium hydroxide; In diethyl ether; dichloromethane; water;