4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one

Base Information

• Chemical Name: 4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one
• CAS No.: 13127-38-3
• Molecular Formula: C₂₇H₂₈Cl₂O
• Molecular Weight: 439.425

Synonyms:4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one

Chemical Property of 4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one

Chemical Property:

Purity/Quality:

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Technology Process of 4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one

There total 2 articles about 4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4-(4-chlorophenylmethylene)-2,6-di-tert-butyl-2,5-cyclohexadien-1-one (70039-17-7) + p-chlorobenzenediazonium tetrafluoroborate (673-41-6) → 4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one (13127-38-3)

Guidance literature:

With ruthenium(III) chloride trihydrate; potassium carbonate; In acetonitrile; at 50 ℃; for 6h; regioselective reaction; Inert atmosphere; Schlenk technique; Sealed tube; Green chemistry;

DOI:10.1021/acs.joc.0c00621

Reference yield:

→ 4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one (13127-38-3)

Guidance literature:

4,4'-Di-chlor-benzophenon, 2,6-Di-t-butyl-phenol;

Reference yield: 83.0%

tert-butylisonitrile (119072-55-8,7188-38-7) + 4-(bis(4-chlorophenyl)methylene)-2,6-di-tert-butylcyclohexa-2,5-dien-1-one (13127-38-3) → 2,2-bis(4-chlorophenyl)-2-(3,5-di-tert-butyl-4-hydroxyphenyl)acetonitrile

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1021/acs.joc.8b01926

upstream raw materials:

4-(4-chlorophenylmethylene)-2,6-di-tert-butyl-2,5-cyclohexadien-1-one

p-chlorobenzenediazonium tetrafluoroborate

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